Measured Data
Specific Heat
Experiments for specific heat [J/(kg K)], or heat capacity, were conducted using a heat flow meter on unconditioned and dried samples at 10 °C, 20 °C, 30 °C and 40 °C.
Unconditioned
Temperature (C) | Specific Heat Mean (J/kg-K) | Standard Deviation (J/kg-K) |
---|---|---|
10.0 | 1533.0 | 366.0 |
20.0 | 1598.0 | 388.0 |
30.0 | 1674.0 | 403.0 |
40.0 | 1741.0 | 417.0 |
Thermal Conductivity
Experiments for thermal conductivity [k] were conducted using a heat flow meter on unconditioned samples at 15 °C and 45 °C.
Unconditioned
Temperature (C) | Conductivity Mean (W/m-K) | Standard Deviation (W/m-K) |
---|---|---|
15.0 | 0.045 | 0.001 |
45.0 | 0.050 | 0.001 |
Mass Loss Rate (MLR)
Initial-mass-normalized mass loss rate [1/s] was measured in the simultaneous thermal analyzer experiments at three heating rates: 3 K/min, 10 K/min, and 30 K/min and mass loss rate [g/s] in the cone calorimeter at three heat fluxes: 25 kW/m2, 50 kW/m2, and 75 kW/m2.
Cone Calorimeter Test Notes:
Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.
Simultaneous Thermal Analyzer
Cone Calorimeter: 25 kW/m2
Cone Calorimeter: 50 kW/m2
Cone Calorimeter: 75 kW/m2
Heat Release Rate Per Unit Area (HRRPUA)
Experiments for heat release per unit area [kW/m2] were conducted on samples conditioned at 20°C and 50% relative humidity using a cone calorimeter at three different heat fluxes: 25 kW/m2, 50 kW/m2, and 75 kW/m2.
Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.
Cone Calorimeter: 50 kW/m2
Cone Calorimeter: 75 kW/m2
Cone Calorimeter: 25 kW/m2
Carbon Monoxide (CO) Yield
Carbon monoxide yield was measured during cone calorimeter experiments conducted at heat fluxes of 25 kW/m2, 50 kW/m2, and 75 kW/m2.
Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.
Incident Heat Flux [kW/m²] | Mean CO Yield [g/g] | CO Yield Std. Dev. [g/g] |
---|---|---|
25 | 0.047 | 0.027 |
50 | 0.026 | 0.002 |
75 | 0.009 | 0.002 |
Specific Heat Release Rate
Experiments for specific heat release rate [W/g], were conducted using a micro-scale combustion calorimeter at a heating rate of 30 K/min.
Derived Data
Effective Heat of Combustion (Δhc)
Effective heat of combustion [MJ/kg] is calculated from data collected in both micro-scale combustion calorimeter experiments and cone calorimeter experiments.
Cone Calorimeter Test Notes:
Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.
Micro-scale Combustion Calorimeter
Value | R1 | R2 | R3 | Mean | Std. Dev. |
---|---|---|---|---|---|
Heat of Combustion (MJ/kg) | 6.7 | 5.79 | 6.29 | 6.26 | 0.37 |
Cone Calorimeter
Incident Heat Flux [kW/m²] | Mean Effective Heat of Combustion [MJ/kg] | Effective Heat of Combustion Std. Dev. [MJ/kg] |
---|---|---|
25 | 10.3 | 0.2 |
50 | 12.1 | 0.4 |
75 | 12.4 | 0.6 |
Band Averaged Emissivity
Band averaged emissivity was calculated from reflectance measurements conducted with an integrating sphere and Fourier transform infrared spectrometer.
Source Temperature [K] | Emissivity | Std. Dev. |
---|---|---|
600.0 | 0.889 | 0.002 |
800.0 | 0.855 | 0.003 |
1000.0 | 0.819 | 0.005 |
1200.0 | 0.783 | 0.007 |
1400.0 | 0.751 | 0.010 |
1600.0 | 0.724 | 0.012 |
1800.0 | 0.702 | 0.015 |
2000.0 | 0.685 | 0.017 |